A Robust Synthesis of 4-substituted 1, 5- Benzodiazepines With the aid of Silica Supported-P2O5 as a Recyclable Catalyst in Solvent-free Conditions

Authors

  • Popat M. Jadhav  Department of Chemistry, Shri Muktanand College, Gangapur, Gangapur, Aurangabad, Maharashtra, India
  • Vijay P. Pagore  Department of Chemistry, Shri Muktanand College, Gangapur, Gangapur, Aurangabad, Maharashtra, India
  • Shivaji B. Munde  Department of Chemistry, Shri Muktanand College, Gangapur, Gangapur, Aurangabad, Maharashtra, India
  • Gautum B. Salve  Department of Chemistry, Shri Muktanand College, Gangapur, Gangapur, Aurangabad, Maharashtra, India
  • Vivekanand B. Jadhav  Department of Chemistry, Shri Muktanand College, Gangapur, Gangapur, Aurangabad, Maharashtra, India

Keywords:

Thermal Decomposition; Electric Conductivity; Solid State; Maleate

Abstract

The possibility of using direct current electric conductivity measurement to study the solid state reactions involved in the preparation zinc oxide from zinc (II) maleate hydrated have been analyzed respectively. The study has been carried out in normal atmosphere. The steps corresponding to dehydration are well resolved in region from room temperature to 260 oC. The final product of decomposition in normal atmosphere was found to be ZnO from zinc maleate. The conductivity measurement was supplemented with the data obtained by chemical analysis; thermal analysis (TGA and DTG) and IR spectroscopy analysis.

References

International Journal of Scientific Research in Science and Technology

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Published

2017-12-31

Issue

Volume 3, Issue 10, November-December-2017

Section

Research Articles

License

Copyright (c) IJSRST

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

How to Cite

[1]
Popat M. Jadhav, Vijay P. Pagore, Shivaji B. Munde, Gautum B. Salve, Vivekanand B. Jadhav, " A Robust Synthesis of 4-substituted 1, 5- Benzodiazepines With the aid of Silica Supported-P2O5 as a Recyclable Catalyst in Solvent-free Conditions, International Journal of Scientific Research in Science and Technology(IJSRST), Online ISSN : 2395-602X, Print ISSN : 2395-6011, Volume 3, Issue 10, pp.154-154, November-December-2017.