A Mercury Free Dopamine Dithiocarbamate Modified Electrode For Pb (II) Determination by Anodic Stripping Voltammetry

Authors

  • J. Kavitha  Department of Analytical Chemistry, University of Madras, Guindy Campus, Chennai, Tamil Nadu, India
  • S. Vasanthi  Department of Analytical Chemistry, University of Madras, Guindy Campus, Chennai, Tamil Nadu, India
  • M. Devendiran  Department of Analytical Chemistry, University of Madras, Guindy Campus, Chennai, Tamil Nadu, India
  • S. Sriman Narayanan  Department of Analytical Chemistry, University of Madras, Guindy Campus, Chennai, Tamil Nadu, India

Keywords:

DDTC, ASV, pH, EDTA, MWCNT

Abstract

A mercury free dopamine dithiocarbomate (DDTC) modified electrode has been proposed for the anodic stripping voltammetric (ASV) determination of Pb (II). DDTC synthesized from dopamine and carbon disulfide. An ethanolic solution of this compound was drop casted on paraffin impregnated graphite electrode to prepare the modified electrode. This electrode was used for Pb (II) determination by ASV. Various parameters such as background electrolyte, pH and preconcentration time were optimized. Under optimized condition, the stripping method provided a linear range from 0.33 to 35 µM for the determination of Pb (II) by ASV. The proposed method is simple, sensitive and selective for the determination of Pb (II) by ASV.

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International Journal of Scientific Research in Science and Technology

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Published

2017-08-31

Issue

Volume 3, Issue 6, July-August-2017

Section

Research Articles

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How to Cite

[1]
J. Kavitha, S. Vasanthi, M. Devendiran, S. Sriman Narayanan, " A Mercury Free Dopamine Dithiocarbamate Modified Electrode For Pb (II) Determination by Anodic Stripping Voltammetry, International Journal of Scientific Research in Science and Technology(IJSRST), Online ISSN : 2395-602X, Print ISSN : 2395-6011, Volume 3, Issue 6, pp.294-301, July-August-2017.