Structural and UV-Vis Diffuse Reflection Spectroscopy Studies of Nanosized Sr0.5Ba0.5Nb2O6 synthesized by Co-Precipitation method

Authors

  • Sanjay B. Nagdeote  Department of Physics, Amolakchand Mahavidyalaya, Yavatmal, Maharashtra, India

DOI:

https://doi.org/10.32628/IJSRST218511

Keywords:

Nanoparticles, TG/DTA, FTIR, Reflectance spectra, XRD

Abstract

The Sr0.5Ba0.5Nb2O6 (SBN-50) is Synthesis by coprecipitation method in nanoscale. TG/DTA shows the reaction and tetragonal phase formation occur at low temperatures, due to which the good homogeneity and morphology of the particles is observed. The average size of the particles was found to be ~ 45 nm. The lattice parameters is found very close to the reported values of single crystals despite method of synthesis and size of the particles. A reflectance spectrum in UV and visible regions shows less reflectance for 337nm and 519nm respectively.

References

  1. R. R. Neurgaonkar, J. R. Oliver and L.E. Cross, Ferroelectrics (1984) 56, 31-36.
  2. T. Volk, L. Ivleva, P. Lykov, N. Polozkov, V. Salobutin, R. Pankrath and M. Wӧhlecke, Optical Materials (2001) 18 179-182.
  3. C. David, T. Granzow, A. Tunyagi, M. Wӧhlecke, T. Woike, K. Betzler, M. Ulex, M. Imalau and R. Pankrath, Phys. Status Solidi A Appl. Res (2004) 201, R49-R52
  4. T. Volk, T. Woike, U. Dorfler, R. Pankrath, L. Ivleva and M. Wӧhlecke, Ferroelectrics (1997) 203, 457-470.
  5. M. Oualla , A. Zegzonti , M. Elaatmani, M. Daoud, D. Mezzane, Y. Gagou and P. Saint-Gregoire  Ferroelectrics (2003) 291 133-
  6. S. Podlozhenov, H. A. Graetsch, J. Schneider, M. Ulex, M. Wӧhlecke and K. Betzler, Acta Crystallographica (2006) B62, 960-965.
  7. M. Ulex, R. Pankrath,and K. Betzler, J. Cryst. Growth, (2004) 271, 128-133.
  8. T. S. Chernaya, T. R. Volk, I. A. Verin, L. I. Ivleva and V. I. Simonov Crystallography Reports (2002) 47, 213-216.
  9. S. Wanmei, L. Shijun, S. Ranran and W. Chunlong, J. Ceramic Processing Research (2011) 12 716-720.
  10. S. N. Mathad and V. Puri, Archives of Physics Research, (2013) 3, 106-115.
  11. S. P. Gaikwad, S. B. Deshpande, Y. Kollam, V. Samual and V. Ravi, Mater Lett. (2004) 58, 3474-6.
  12. S. R. Dhage, Y. Kollam, S. B. Deshpande and V. Ravi, Mater Res. Bull. (2003) 38, 1601-1605.
  13. A. V. Murugan, A. B. Gaikwad, V. Samual and V. Ravi, Bull. Mater. Sci. (2006), 29, 221-223.
  14. F.A. Al-Newaiser, S. A. Al-Thabaiti, A.O. Al-Youbi, A. Y. Obaid and M. A. Gabal, Thermal decomposition kinetics of strontium oxalate, Chem Pap.( 2007) 61, 370-375.
  15. M. I. Diaz-Guemes, T. Gonzalezcarreno, C.J. Serna, Spectrochim. Acta. A 45 (1989) 589.
  16. W. Bollmann, H. J. Stohr, Phys. Stat. Sol. A 39 (1977) 477.
  17. A. E. Morales, E. S. Mora, U. Pal, Rev. Mex. Fis. 53 (2007) 18.
  18. S. M. Kaczmarek, M. Orowski, T. Skibinski, A. Jasik, L. I. Ivleva, Rev. Adv. Mater.Sci. 23 (2010) 80.

International Journal of Scientific Research in Science and Technology

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Published

2021-10-30

Issue

Volume 8, Issue 5, September-October-2021

Section

Research Articles

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How to Cite

[1]
Sanjay B. Nagdeote "Structural and UV-Vis Diffuse Reflection Spectroscopy Studies of Nanosized Sr0.5Ba0.5Nb2O6 synthesized by Co-Precipitation method" International Journal of Scientific Research in Science and Technology(IJSRST), Online ISSN : 2395-602X, Print ISSN : 2395-6011,Volume 8, Issue 5, pp.78-83, September-October-2021. Available at doi : https://doi.org/10.32628/IJSRST218511