Synthesis and Structural Characterization of Nickel Oxide-Polyaniline Nanocomposite

Authors

  • A. I. Nandapure  Department of Physics, Yeshwant Mahavidyalaya, Wardha, Maharashtra, India
  • B. I. Nandapure  Department of Physics, Sindhu Mahavidyalaya, Nagpur, Maharashtra, India
  • S. B. Kondawar  Department of Physics, RTM Nagpur University, Nagpur, Maharashtra, India

Keywords:

Conducting Polymer, Polyaniline, Nano Nickel Oxide, Nanocomposite, TEM, FTIR.

Abstract

Nickel oxide polyaniline nanocomposite (NiO-PANI) was synthesized by in situ polymerization technique in sulphuric acid medium with ammonium persulphate as an oxidizing agent in the presence of synthesized nanoparticles NiO as reinforcing filler so as to study the effect of filler nanoparticles on the properties of the conducting polyaniline. The synthesized nanocomposite was characterized by Transmission Electron Microscopy (TEM), Fourier transform infrared spectroscopy (FTIR), Ultraviolet visible spectroscopy (UV). TEM pattern shows uniform NiO-PANI nanoparticles having diameter 20nm. FTIR spectroscopy shows that NiO nanoparticles get electrostatically bound to the specific sites of polyaniline. UV- visible spectroscopy shows that coating of NiO nanoparticles on PANI backbone.

References

  1. Zhang Q, Liu F, Li L, et al. 2011. Journal of  Nanoparticle Research. ISSN No: 1572-896X. DOI : 10.1007/s11051-010-0070-8.
  2. Kondawar SB, Thakare SR, Bompilwar SD, et al.2009. International  Journal of Modern Physics  B (June 2009) ISSN No: 1793-6578. DOI : 10.1142/s0217979209052583.
  3. Umare SS, Shambharkar BH and Ningthoujam RS. 2010. Synthetic Metal 2010. ISSN No: 0379-6779. DOI : 10.1016/201006015.
  4. Aphesteguy JC and Jacobo SE. 2004. Physican B: Condensed Matter. ISSN No: 0921-4526. DOI : 10.1016/200409053.
  5. Song G, Han J and Guo R. 2007. . Synthetic Metal. ISSN No: 0379-6779. DOI : 10.1016/200612007.
  6. Aleahmad M, Ghafouri H and Taleghani H. 2011.Synthetic Metal 2011. ISSN No: 0379-6779. DOI : 10.1016/201103005.
  7. Sharma BK, Gupta AK, Kharea N, et al. 2009. Synthetic  Metal 2009. ISSN No: 0379-6779. DOI : 10.1016/200810010.
  8. Zhao YP, Cai ZS, Zhou ZY, et al. 2011. Thin Solid Films. ISSN No: 0040-6090. DOI : 10.1016/201102088.
  9. Zhong H, Yuan R, Chai Y, et al. 2011. Talanta. ISSN No: 0039-9140. DOI : 10.1016/201103040.
  10. Chakraborty G, Guatak S, Meikap AK, Blau Werner J, et al. 2010. Journal of Polymer Science Part B: Polymer Physics. ISSN No: 1099-0488. DOI : 10.1002/polb.22042.
  11. Ghatak S, Chakraborty G, Meikap AK, et al. 2011. Journal of Applied Polymer Science. ISSN No: 1097-4628. DOI : 10.1002/app.31962.
  12. Nandapure B.I.  Kondawar S.B.  Salunkhe M.Y. Nandapure A.I. Journal of advanced material letters. ISSN No: 0976-3961. DOI : 10.5185/amlett.20125348.
  13. Yanni Qi, Jian Zhang, Shujun Qiu, Lixian Sun, Fen Xu, Min Zhu, Liuzhang Ouyang and Dalin Sun.  2009. Journal of  Thermal Analysis and Calorimetry. ISSN No: 1572-8943. DOI : 10.1007/s10973-009-0298-7.
  14. Ying Wang, Ya-Fei Zhang, Hai-Rong Liu, Shen-Jiang Yu, Qi-Zong Qin. 2003. Journal of Electrochimica Acta. ISSN No: 0013-4686. DOI : 10.1016/S0013-4686(03)00612-1.
  15. Romero R, Martin F, Ramos-Barrado JR, Leinen D. 2010. Journal of Thin Solid Films. ISSN No: 0040-6090. DOI : 10.1016/j.tsf 200912016.
  16. Kemari M.El., Nagy N., Mehasseb I-El. 2013. Journal of material science in semiconductor processing. ISSN No: 1369-8001. DOI : 10.1016/j.mssp.201305018.
  17. Umare SS, Shambharkar BH. 2011.Journal of Applied Polymer Science. ISSN No: 1097-4628. DOI : 10.1002/app.31962.
  18. Salavati-Niasari, M. Mohandes, F. Davar, F. Mazaheri, M. Monemzadeh, M. Yavarinia, N. 2009.  Journal of Inorganica chimica acta. ISSN No: 0020-1693. DOI : 10.1016/j.ica.200904025.
  19. Salavati-Niasari. M.; Mir, N. Davar, F.2009. Journal of Polyhedron. ISSN No: 0277-5387. DOI : 10.1016/j.poly.200901026.
  20. Barve A.K. Gadegone S.M. Lanjewar M.R. Lanjewar R.B. 2014. International journal of Engineering research and applications. ISSN No: 2248-9622.

International Journal of Scientific Research in Science and Technology

Downloads

Published

2018-01-30

Issue

Volume 4, Issue 1, January-February-2018

Section

Research Articles

License

Copyright (c) IJSRST

Creative Commons License

This work is licensed under a Creative Commons Attribution 4.0 International License.

How to Cite

[1]
A. I. Nandapure, B. I. Nandapure, S. B. Kondawar "Synthesis and Structural Characterization of Nickel Oxide-Polyaniline Nanocomposite" International Journal of Scientific Research in Science and Technology(IJSRST), Online ISSN : 2395-602X, Print ISSN : 2395-6011,Volume 4, Issue 1, pp.11-14, January-February-2018.